Detection Summary
Client: Rock Engineering & Testing Lab., Inc.
TestAmerica Job ID: 560-27205-1
Project/Site: G111204 Prop'd Bahia Grande Restoration
Client Sample ID: B-1; 1.0'-5.0'
Lab Sample ID: 560-27205-1
Analyte
Result Qualifier
Unit
Dil Fac D Method
Prep Type
Toluene
0.00057 J
RL
0.0044
mg/Kg
1
8260B
Total/NA
MDL
0.00049
Bis(2-ethylhexyl) phthalate
0.096 J
0.33
0.017 mg/Kg
1
8270C
Total/NA
Arsenic
3.3
0.21
0.043 mg/Kg
1
6020
Total/NA
Barium
120
0.43
0.19 mg/Kg
2
6020
Total/NA
Cadmium
0.10 J
0.21
0.062 mg/Kg
1
6020
Total/NA
Chromium
7.8
0.21
0.096 mg/Kg
1
6020
Total/NA
Lead
7.2
0.43
0.18 mg/Kg
1
6020
Total/NA
Selenium
0.14 J
0.21
0.037 mg/Kg
1
6020
Total/NA
Silver
0.16 J
0.21
0.059 mg/Kg
1
6020
Total/NA
Client Sample ID: B-2; 6.0'-10.0'
Lab Sample ID: 560-27205-2
Analyte
Result Qualifier
Unit
Dil Fac D Method
Prep Type
Arsenic
3.0
RL
0.22
mg/Kg
1
6020
Total/NA
MDL
0.043
Barium
120
0.43
0.19 mg/Kg
2
6020
Total/NA
Cadmium
0.13 J
0.22
0.062 mg/Kg
1
6020
Total/NA
Chromium
6.9
0.22
0.097 mg/Kg
1
6020
Total/NA
Lead
5.3
0.43
0.18 mg/Kg
1
6020
Total/NA
Selenium
0.17 J
0.22
0.038 mg/Kg
1
6020
Total/NA
Client Sample ID: B-3; 1.0'-5.0'
Lab Sample ID: 560-27205-3
Analyte
Result Qualifier
Unit
Dil Fac D Method
Prep Type
Toluene
0.00053 J
RL
0.0045
mg/Kg
1
8260B
Total/NA
MDL
0.00050
Arsenic
3.2
0.21
0.043 mg/Kg
1
6020
Total/NA
Barium
89
0.43
0.19 mg/Kg
2
6020
Total/NA
Cadmium
0.13 J
0.21
0.062 mg/Kg
1
6020
Total/NA
Chromium
5.5
0.21
0.096 mg/Kg
1
6020
Total/NA
Lead
5.6
0.43
0.18 mg/Kg
1
6020
Total/NA
Selenium
0.13 J
0.21
0.037 mg/Kg
1
6020
Total/NA
Client Sample ID: B-4; 6.0'-10.0'
Lab Sample ID: 560-27205-4
Analyte
Result Qualifier
Unit
Dil Fac D Method
Prep Type
Toluene
0.00062 J
RL
0.0045
mg/Kg
1
8260B
Total/NA
MDL
0.00051
Over C12-C28
13 J
50
10 mg/Kg
1
TX 1005
Total/NA
Total Petroleum Hydrocarbons
(C6-C35)
13 J B
50
10 mg/Kg
1
TX 1005
Total/NA
Arsenic
4.6
0.20
0.039 mg/Kg
1
6020
Total/NA
Barium
170
0.39
0.17 mg/Kg
2
6020
Total/NA
Cadmium
0.17 J
0.20
0.057 mg/Kg
1
6020
Total/NA
Chromium
8.2
0.20
0.088 mg/Kg
1
6020
Total/NA
Lead
8.8
0.39
0.16 mg/Kg
1
6020
Total/NA
Selenium
0.24
0.20
0.034 mg/Kg
1
6020
Total/NA
Mercury
0.013 J
0.12
0.011 mg/Kg
1
7471A
Total/NA
TestAmerica Corpus Christi
Page 4 of 40
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Client Sample Results
Client: Rock Engineering & Testing Lab., Inc.
TestAmerica Job ID: 560-27205-1
Project/Site: G111204 Prop'd Bahia Grande Restoration
Client Sample ID: B-1; 1.0'-5.0'
Lab Sample ID: 560-27205-1
Date Collected: 07/22/11 12:30
Matrix: Solid
Date Received: 07/22/11 12:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Dichlorodifluoromethane
<0.00064
0.0044
0.00064 mg/Kg
07/25/11 13:23
1
Analyte
Chloromethane
<0.0011
0.0044
0.0011 mg/Kg
07/25/11 13:23
1
Vinyl chloride
<0.00053
0.0044
0.00053 mg/Kg
07/25/11 13:23
1
Bromomethane
<0.00097
0.0044
0.00097 mg/Kg
07/25/11 13:23
1
Chloroethane
<0.00023
0.0044
0.00023 mg/Kg
07/25/11 13:23
1
Trichlorofluoromethane
<0.00044
0.0044
0.00044 mg/Kg
07/25/11 13:23
1
Ethyl ether
<0.00015
0.0044
0.00015 mg/Kg
07/25/11 13:23
1
1,1-Dichloroethene
<0.00017
0.0044
0.00017 mg/Kg
07/25/11 13:23
1
Carbon disulfide
<0.00088
0.0044
0.00088 mg/Kg
07/25/11 13:23
1
Iodomethane
<0.00071
0.0044
0.00071 mg/Kg
07/25/11 13:23
1
Methylene Chloride
<0.0044
0.022
0.0044 mg/Kg
07/25/11 13:23
1
Acetone
<0.0063
0.044
0.0063 mg/Kg
07/25/11 13:23
1
trans-1,2-Dichloroethene
<0.00044
0.0044
0.00044 mg/Kg
07/25/11 13:23
1
Methyl tert-butyl ether
<0.00054
0.0044
0.00054 mg/Kg
07/25/11 13:23
1
Acetonitrile
<0.033
0.044
0.033 mg/Kg
07/25/11 13:23
1
1,1-Dichloroethane
<0.00052
0.0044
0.00052 mg/Kg
07/25/11 13:23
1
Vinyl acetate
<0.00097
0.0044
0.00097 mg/Kg
07/25/11 13:23
1
cis-1,2-Dichloroethene
<0.00050
0.0044
0.00050 mg/Kg
07/25/11 13:23
1
2,2-Dichloropropane
<0.00074
0.0044
0.00074 mg/Kg
07/25/11 13:23
1
Chloroform
<0.00077
0.0044
0.00077 mg/Kg
07/25/11 13:23
1
Ethyl acetate
<0.0011
0.0044
0.0011 mg/Kg
07/25/11 13:23
1
Carbon tetrachloride
<0.00045
0.0044
0.00045 mg/Kg
07/25/11 13:23
1
1,1,1-Trichloroethane
<0.00062
0.0044
0.00062 mg/Kg
07/25/11 13:23
1
1,1-Dichloropropene
<0.00046
0.0044
0.00046 mg/Kg
07/25/11 13:23
1
Benzene
<0.00020
0.0044
0.00020 mg/Kg
07/25/11 13:23
1
1,2-Dichloroethane
<0.00046
0.0044
0.00046 mg/Kg
07/25/11 13:23
1
Trichloroethene
<0.00025
0.0044
0.00025 mg/Kg
07/25/11 13:23
1
Dibromomethane
<0.00063
0.0044
0.00063 mg/Kg
07/25/11 13:23
1
1,2-Dichloropropane
<0.00013
0.0044
0.00013 mg/Kg
07/25/11 13:23
1
Dichlorobromomethane
<0.00017
0.0044
0.00017 mg/Kg
07/25/11 13:23
1
Methyl methacrylate
<0.00097
0.0044
0.00097 mg/Kg
07/25/11 13:23
1
1,4-Dioxane
<0.017
0.088
0.017 mg/Kg
07/25/11 13:23
1
cis-1,3-Dichloropropene
<0.00012
0.0044
0.00012 mg/Kg
07/25/11 13:23
1
Toluene
0.00057 J
0.0044
0.00049 mg/Kg
07/25/11 13:23
1
2-Nitropropane
<0.00046
0.0044
0.00046 mg/Kg
07/25/11 13:23
1
4-Methyl-2-pentanone (MIBK)
<0.00082
0.0044
0.00082 mg/Kg
07/25/11 13:23
1
trans-1,3-Dichloropropene
<0.00046
0.0044
0.00046 mg/Kg
07/25/11 13:23
1
Tetrachloroethene
<0.00065
0.0044
0.00065 mg/Kg
07/25/11 13:23
1
Ethyl methacrylate
<0.00045
0.0044
0.00045 mg/Kg
07/25/11 13:23
1
1,1,2-Trichloroethane
<0.00044
0.0044
0.00044 mg/Kg
07/25/11 13:23
1
Chlorodibromomethane
<0.00056
0.0044
0.00056 mg/Kg
07/25/11 13:23
1
1,3-Dichloropropane
<0.00021
0.0044
0.00021 mg/Kg
07/25/11 13:23
1
Ethylene Dibromide
<0.00015
0.0044
0.00015 mg/Kg
07/25/11 13:23
1
2-Hexanone
<0.0011
0.0044
0.0011 mg/Kg
07/25/11 13:23
1
Chlorobenzene
<0.00020
0.0044
0.00020 mg/Kg
07/25/11 13:23
1
Ethylbenzene
<0.00019
0.0044
0.00019 mg/Kg
07/25/11 13:23
1
Bromoform
<0.00045
0.0044
0.00045 mg/Kg
07/25/11 13:23
1
Styrene
<0.00018
0.0044
0.00018 mg/Kg
07/25/11 13:23
1
1,1,2,2-Tetrachloroethane
<0.00034
0.0044
0.00034 mg/Kg
07/25/11 13:23
1
1,2,3-Trichloropropane
<0.00067
0.0044
0.00067 mg/Kg
07/25/11 13:23
1
TestAmerica Corpus Christi
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Client Sample Results
Client: Rock Engineering & Testing Lab., Inc.
TestAmerica Job ID: 560-27205-1
Project/Site: G111204 Prop'd Bahia Grande Restoration
Client Sample ID: B-1; 1.0'-5.0'
Lab Sample ID: 560-27205-1
Date Collected: 07/22/11 12:30
Matrix: Solid
Date Received: 07/22/11 12:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,3,5-Trimethylbenzene
<0.00019
0.0044
0.00019 mg/Kg
07/25/11 13:23
1
Analyte
1,2,4-Trimethylbenzene
<0.00018
0.0044
0.00018 mg/Kg
07/25/11 13:23
1
1,2,3-Trichlorobenzene
<0.00039
0.0044
0.00039 mg/Kg
07/25/11 13:23
1
2-Butanone (MEK)
<0.00088
0.0044
0.00088 mg/Kg
07/25/11 13:23
1
1,1,2-Trichloro-1,2,2-trifluoroethane
<0.00059
0.0044
0.00059 mg/Kg
07/25/11 13:23
1
Xylenes, Total
<0.00032
0.013
0.00032 mg/Kg
07/25/11 13:23
1
% Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Dibromofluoromethane (Surr)
85
63
-
136
07/25/11 13:23
1
Surrogate
1,2-Dichloroethane-d4 (Surr)
95
70
-
152
07/25/11 13:23
1
Toluene-d8 (Surr)
99
69
-
139
07/25/11 13:23
1
4-Bromofluorobenzene (Surr)
96
61
-
130
07/25/11 13:23
1
Method: 8270C - Semivolatile Organic Compounds (GC/MS)
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Phenol
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Analyte
Bis(2-chloroethyl)ether
<0.037
0.33
0.037 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
2-Chlorophenol
<0.028
0.33
0.028 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
1,3-Dichlorobenzene
<0.044
0.33
0.044 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
1,4-Dichlorobenzene
<0.046
0.33
0.046 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Benzyl alcohol
<0.024
0.33
0.024 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
1,2-Dichlorobenzene
<0.052
0.33
0.052 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
2-Methylphenol
<0.033
0.33
0.033 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
3 & 4 Methylphenol
<0.050
0.67
0.050 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
N-Nitrosodi-n-propylamine
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Hexachloroethane
<0.050
0.33
0.050 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Nitrobenzene
<0.036
0.33
0.036 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Isophorone
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
2-Nitrophenol
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
2,4-Dimethylphenol
<0.020
0.33
0.020 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Bis(2-chloroethoxy)methane
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
2,4-Dichlorophenol
<0.023
0.33
0.023 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
1,2,4-Trichlorobenzene
<0.046
0.33
0.046 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Naphthalene
<0.042
0.33
0.042 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
4-Chloroaniline
<0.047
0.33
0.047 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Hexachlorobutadiene
<0.045
0.33
0.045 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
4-Chloro-3-methylphenol
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
2-Methylnaphthalene
<0.031
0.33
0.031 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Hexachlorocyclopentadiene
<0.10
0.33
0.10 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
2,4,6-Trichlorophenol
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
2,4,5-Trichlorophenol
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
2-Chloronaphthalene
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
2-Nitroaniline
<0.022
0.33
0.022 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Dimethyl phthalate
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Acenaphthylene
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
2,6-Dinitrotoluene
<0.050
0.33
0.050 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
3-Nitroaniline
<0.050
0.33
0.050 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Acenaphthene
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
2,4-Dinitrophenol
<0.10
0.33
0.10 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
4-Nitrophenol
<0.030
0.33
0.030 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
TestAmerica Corpus Christi
Page 6 of 40
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Client Sample Results
Client: Rock Engineering & Testing Lab., Inc.
TestAmerica Job ID: 560-27205-1
Project/Site: G111204 Prop'd Bahia Grande Restoration
Client Sample ID: B-1; 1.0'-5.0'
Lab Sample ID: 560-27205-1
Date Collected: 07/22/11 12:30
Matrix: Solid
Date Received: 07/22/11 12:40
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Dibenzofuran
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Analyte
2,4-Dinitrotoluene
<0.021
0.33
0.021 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Diethyl phthalate
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Fluorene
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
4-Chlorophenyl phenyl ether
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
4-Nitroaniline
<0.028
0.33
0.028 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
4,6-Dinitro-2-methylphenol
<0.050
0.33
0.050 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
N-Nitrosodiphenylamine
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
4-Bromophenyl phenyl ether
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Hexachlorobenzene
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Phenanthrene
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Anthracene
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Di-n-butyl phthalate
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Fluoranthene
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Pyrene
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Butyl benzyl phthalate
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Benzo[a]anthracene
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Chrysene
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Bis(2-ethylhexyl) phthalate
0.096 J
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Di-n-octyl phthalate
<0.019
0.33
0.019 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Benzo[b]fluoranthene
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Benzo[k]fluoranthene
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Benzo[a]pyrene
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Indeno[1,2,3-cd]pyrene
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Dibenz(a,h)anthracene
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Benzo[g,h,i]perylene
<0.017
0.33
0.017 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
3,3'-Dichlorobenzidine
<0.050
0.33
0.050 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
Pentachlorophenol
<0.10
0.33
0.10 mg/Kg
07/25/11 13:21
07/26/11 16:46
1
% Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorophenol
77
48
-
130
07/25/11 13:21
07/26/11 16:46
1
Surrogate
Phenol-d5
81
56
-
130
07/25/11 13:21
07/26/11 16:46
1
Nitrobenzene-d5
77
48
-
130
07/25/11 13:21
07/26/11 16:46
1
2-Fluorobiphenyl
78
57
-
130
07/25/11 13:21
07/26/11 16:46
1
2,4,6-Tribromophenol
91
30
-
131
07/25/11 13:21
07/26/11 16:46
1
Terphenyl-d14
91
58
-
130
07/25/11 13:21
07/26/11 16:46
1
Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Aroclor 1016
<0.0052
0.034
0.0052 mg/Kg
07/25/11 07:22
07/25/11 14:43
1
Analyte
Aroclor 1221
<0.0052
0.034
0.0052 mg/Kg
07/25/11 07:22
07/25/11 14:43
1
Aroclor 1232
<0.0052
0.034
0.0052 mg/Kg
07/25/11 07:22
07/25/11 14:43
1
Aroclor 1242
<0.0052
0.034
0.0052 mg/Kg
07/25/11 07:22
