Detection Summary
Client: Rock Engineering & Testing Lab., Inc.
TestAmerica Job ID: 560-27205-1
Project/Site: G111204 Prop'd Bahia Grande Restoration
Client Sample ID: B-1; 1.0'-5.0'
Lab Sample ID: 560-27205-1
Analyte
Result Qualifier
Unit
Dil Fac D Method
Prep Type
Toluene
0.00057 J
RL
0.0044
mg/Kg
1
8260B
Total/NA
MDL
0.00049
Bis(2-ethylhexyl) phthalate
0.096 J
0.33
0.017 mg/Kg
1
8270C
Total/NA
Arsenic
3.3
0.21
0.043 mg/Kg
1
6020
Total/NA
Barium
120
0.43
0.19 mg/Kg
2
6020
Total/NA
Cadmium
0.10 J
0.21
0.062 mg/Kg
1
6020
Total/NA
Chromium
7.8
0.21
0.096 mg/Kg
1
6020
Total/NA
Lead
7.2
0.43
0.18 mg/Kg
1
6020
Total/NA
Selenium
0.14 J
0.21
0.037 mg/Kg
1
6020
Total/NA
Silver
0.16 J
0.21
0.059 mg/Kg
1
6020
Total/NA
Client Sample ID: B-2; 6.0'-10.0'
Lab Sample ID: 560-27205-2
Analyte
Result Qualifier
Unit
Dil Fac D Method
Prep Type
Arsenic
3.0
RL
0.22
mg/Kg
1
6020
Total/NA
MDL
0.043
Barium
120
0.43
0.19 mg/Kg
2
6020
Total/NA
Cadmium
0.13 J
0.22
0.062 mg/Kg
1
6020
Total/NA
Chromium
6.9
0.22
0.097 mg/Kg
1
6020
Total/NA
Lead
5.3
0.43
0.18 mg/Kg
1
6020
Total/NA
Selenium
0.17 J
0.22
0.038 mg/Kg
1
6020
Total/NA
Client Sample ID: B-3; 1.0'-5.0'
Lab Sample ID: 560-27205-3
Analyte
Result Qualifier
Unit
Dil Fac D Method
Prep Type
Toluene
0.00053 J
RL
0.0045
mg/Kg
1
8260B
Total/NA
MDL
0.00050
Arsenic
3.2
0.21
0.043 mg/Kg
1
6020
Total/NA
Barium
89
0.43
0.19 mg/Kg
2
6020
Total/NA
Cadmium
0.13 J
0.21
0.062 mg/Kg
1
6020
Total/NA
Chromium
5.5
0.21
0.096 mg/Kg
1
6020
Total/NA
Lead
5.6
0.43
0.18 mg/Kg
1
6020
Total/NA
Selenium
0.13 J
0.21
0.037 mg/Kg
1
6020
Total/NA
Client Sample ID: B-4; 6.0'-10.0'
Lab Sample ID: 560-27205-4
Analyte
Result Qualifier
Unit
Dil Fac D Method
Prep Type
Toluene
0.00062 J
RL
0.0045
mg/Kg
1
8260B
Total/NA
MDL
0.00051
Over C12-C28
13 J
50
10 mg/Kg
1
TX 1005
Total/NA
Total Petroleum Hydrocarbons
(C6-C35)
13 J B
50
10 mg/Kg
1
TX 1005
Total/NA
Arsenic
4.6
0.20
0.039 mg/Kg
1
6020
Total/NA
Barium
170
0.39
0.17 mg/Kg
2
6020
Total/NA
Cadmium
0.17 J
0.20
0.057 mg/Kg
1
6020
Total/NA
Chromium
8.2
0.20
0.088 mg/Kg
1
6020
Total/NA
Lead
8.8
0.39
0.16 mg/Kg
1
6020
Total/NA
Selenium
0.24
0.20
0.034 mg/Kg
1
6020
Total/NA
Mercury
0.013 J
0.12
0.011 mg/Kg
1
7471A
Total/NA
TestAmerica Corpus Christi
Page 4 of 40
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Client Sample Results
Client: Rock Engineering & Testing Lab., Inc.
TestAmerica Job ID: 560-27205-1
Project/Site: G111204 Prop'd Bahia Grande Restoration
Client Sample ID: B-4; 6.0'-10.0'
Lab Sample ID: 560-27205-4
Date Collected: 07/22/11 12:36
Matrix: Solid
Date Received: 07/22/11 12:40
Method: 8260B - Volatile Organic Compounds (GC/MS)
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Dichlorodifluoromethane
<0.00066
0.0045
0.00066 mg/Kg
07/25/11 14:13
1
Analyte
Chloromethane
<0.0011
0.0045
0.0011 mg/Kg
07/25/11 14:13
1
Vinyl chloride
<0.00054
0.0045
0.00054 mg/Kg
07/25/11 14:13
1
Bromomethane
<0.0010
0.0045
0.0010 mg/Kg
07/25/11 14:13
1
Chloroethane
<0.00024
0.0045
0.00024 mg/Kg
07/25/11 14:13
1
Trichlorofluoromethane
<0.00045
0.0045
0.00045 mg/Kg
07/25/11 14:13
1
Ethyl ether
<0.00015
0.0045
0.00015 mg/Kg
07/25/11 14:13
1
1,1-Dichloroethene
<0.00017
0.0045
0.00017 mg/Kg
07/25/11 14:13
1
Carbon disulfide
<0.00091
0.0045
0.00091 mg/Kg
07/25/11 14:13
1
Iodomethane
<0.00073
0.0045
0.00073 mg/Kg
07/25/11 14:13
1
Methylene Chloride
<0.0045
0.023
0.0045 mg/Kg
07/25/11 14:13
1
Acetone
<0.0065
0.045
0.0065 mg/Kg
07/25/11 14:13
1
trans-1,2-Dichloroethene
<0.00045
0.0045
0.00045 mg/Kg
07/25/11 14:13
1
Methyl tert-butyl ether
<0.00055
0.0045
0.00055 mg/Kg
07/25/11 14:13
1
Acetonitrile
<0.034
0.045
0.034 mg/Kg
07/25/11 14:13
1
1,1-Dichloroethane
<0.00054
0.0045
0.00054 mg/Kg
07/25/11 14:13
1
Vinyl acetate
<0.0010
0.0045
0.0010 mg/Kg
07/25/11 14:13
1
cis-1,2-Dichloroethene
<0.00052
0.0045
0.00052 mg/Kg
07/25/11 14:13
1
2,2-Dichloropropane
<0.00076
0.0045
0.00076 mg/Kg
07/25/11 14:13
1
Chloroform
<0.00079
0.0045
0.00079 mg/Kg
07/25/11 14:13
1
Ethyl acetate
<0.0011
0.0045
0.0011 mg/Kg
07/25/11 14:13
1
Carbon tetrachloride
<0.00046
0.0045
0.00046 mg/Kg
07/25/11 14:13
1
1,1,1-Trichloroethane
<0.00064
0.0045
0.00064 mg/Kg
07/25/11 14:13
1
1,1-Dichloropropene
<0.00047
0.0045
0.00047 mg/Kg
07/25/11 14:13
1
Benzene
<0.00021
0.0045
0.00021 mg/Kg
07/25/11 14:13
1
1,2-Dichloroethane
<0.00047
0.0045
0.00047 mg/Kg
07/25/11 14:13
1
Trichloroethene
<0.00025
0.0045
0.00025 mg/Kg
07/25/11 14:13
1
Dibromomethane
<0.00064
0.0045
0.00064 mg/Kg
07/25/11 14:13
1
1,2-Dichloropropane
<0.00014
0.0045
0.00014 mg/Kg
07/25/11 14:13
1
Dichlorobromomethane
<0.00017
0.0045
0.00017 mg/Kg
07/25/11 14:13
1
Methyl methacrylate
<0.0010
0.0045
0.0010 mg/Kg
07/25/11 14:13
1
1,4-Dioxane
<0.017
0.091
0.017 mg/Kg
07/25/11 14:13
1
cis-1,3-Dichloropropene
<0.00013
0.0045
0.00013 mg/Kg
07/25/11 14:13
1
Toluene
0.00062 J
0.0045
0.00051 mg/Kg
07/25/11 14:13
1
2-Nitropropane
<0.00047
0.0045
0.00047 mg/Kg
07/25/11 14:13
1
4-Methyl-2-pentanone (MIBK)
<0.00084
0.0045
0.00084 mg/Kg
07/25/11 14:13
1
trans-1,3-Dichloropropene
<0.00047
0.0045
0.00047 mg/Kg
07/25/11 14:13
1
Tetrachloroethene
<0.00067
0.0045
0.00067 mg/Kg
07/25/11 14:13
1
Ethyl methacrylate
<0.00046
0.0045
0.00046 mg/Kg
07/25/11 14:13
1
1,1,2-Trichloroethane
<0.00045
0.0045
0.00045 mg/Kg
07/25/11 14:13
1
Chlorodibromomethane
<0.00058
0.0045
0.00058 mg/Kg
07/25/11 14:13
1
1,3-Dichloropropane
<0.00022
0.0045
0.00022 mg/Kg
07/25/11 14:13
1
Ethylene Dibromide
<0.00015
0.0045
0.00015 mg/Kg
07/25/11 14:13
1
2-Hexanone
<0.0011
0.0045
0.0011 mg/Kg
07/25/11 14:13
1
Chlorobenzene
<0.00021
0.0045
0.00021 mg/Kg
07/25/11 14:13
1
Ethylbenzene
<0.00020
0.0045
0.00020 mg/Kg
07/25/11 14:13
1
Bromoform
<0.00046
0.0045
0.00046 mg/Kg
07/25/11 14:13
1
Styrene
<0.00018
0.0045
0.00018 mg/Kg
07/25/11 14:13
1
1,1,2,2-Tetrachloroethane
<0.00034
0.0045
0.00034 mg/Kg
07/25/11 14:13
1
1,2,3-Trichloropropane
<0.00069
0.0045
0.00069 mg/Kg
07/25/11 14:13
1
TestAmerica Corpus Christi
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Client Sample Results
Client: Rock Engineering & Testing Lab., Inc.
TestAmerica Job ID: 560-27205-1
Project/Site: G111204 Prop'd Bahia Grande Restoration
Client Sample ID: B-4; 6.0'-10.0'
Lab Sample ID: 560-27205-4
Date Collected: 07/22/11 12:36
Matrix: Solid
Date Received: 07/22/11 12:40
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,3,5-Trimethylbenzene
<0.00019
0.0045
0.00019 mg/Kg
07/25/11 14:13
1
Analyte
1,2,4-Trimethylbenzene
<0.00018
0.0045
0.00018 mg/Kg
07/25/11 14:13
1
1,2,3-Trichlorobenzene
<0.00040
0.0045
0.00040 mg/Kg
07/25/11 14:13
1
2-Butanone (MEK)
<0.00091
0.0045
0.00091 mg/Kg
07/25/11 14:13
1
1,1,2-Trichloro-1,2,2-trifluoroethane
<0.00061
0.0045
0.00061 mg/Kg
07/25/11 14:13
1
Xylenes, Total
<0.00033
0.014
0.00033 mg/Kg
07/25/11 14:13
1
% Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Dibromofluoromethane (Surr)
91
63
-
136
07/25/11 14:13
1
Surrogate
1,2-Dichloroethane-d4 (Surr)
96
70
-
152
07/25/11 14:13
1
Toluene-d8 (Surr)
100
69
-
139
07/25/11 14:13
1
4-Bromofluorobenzene (Surr)
95
61
-
130
07/25/11 14:13
1
Method: 8270C - Semivolatile Organic Compounds (GC/MS)
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Phenol
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Analyte
Bis(2-chloroethyl)ether
<0.038
0.34
0.038 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
2-Chlorophenol
<0.028
0.34
0.028 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
1,3-Dichlorobenzene
<0.045
0.34
0.045 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
1,4-Dichlorobenzene
<0.047
0.34
0.047 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Benzyl alcohol
<0.025
0.34
0.025 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
1,2-Dichlorobenzene
<0.053
0.34
0.053 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
2-Methylphenol
<0.034
0.34
0.034 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
3 & 4 Methylphenol
<0.051
0.69
0.051 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
N-Nitrosodi-n-propylamine
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Hexachloroethane
<0.051
0.34
0.051 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Nitrobenzene
<0.037
0.34
0.037 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Isophorone
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
2-Nitrophenol
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
2,4-Dimethylphenol
<0.021
0.34
0.021 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Bis(2-chloroethoxy)methane
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
2,4-Dichlorophenol
<0.023
0.34
0.023 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
1,2,4-Trichlorobenzene
<0.047
0.34
0.047 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Naphthalene
<0.043
0.34
0.043 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
4-Chloroaniline
<0.048
0.34
0.048 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Hexachlorobutadiene
<0.046
0.34
0.046 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
4-Chloro-3-methylphenol
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
2-Methylnaphthalene
<0.032
0.34
0.032 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Hexachlorocyclopentadiene
<0.10
0.34
0.10 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
2,4,6-Trichlorophenol
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
2,4,5-Trichlorophenol
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
2-Chloronaphthalene
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
2-Nitroaniline
<0.023
0.34
0.023 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Dimethyl phthalate
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Acenaphthylene
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
2,6-Dinitrotoluene
<0.051
0.34
0.051 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
3-Nitroaniline
<0.051
0.34
0.051 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Acenaphthene
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
2,4-Dinitrophenol
<0.10
0.34
0.10 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
4-Nitrophenol
<0.031
0.34
0.031 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
TestAmerica Corpus Christi
Page 17 of 40
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Client Sample Results
Client: Rock Engineering & Testing Lab., Inc.
TestAmerica Job ID: 560-27205-1
Project/Site: G111204 Prop'd Bahia Grande Restoration
Client Sample ID: B-4; 6.0'-10.0'
Lab Sample ID: 560-27205-4
Date Collected: 07/22/11 12:36
Matrix: Solid
Date Received: 07/22/11 12:40
Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Dibenzofuran
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Analyte
2,4-Dinitrotoluene
<0.022
0.34
0.022 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Diethyl phthalate
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Fluorene
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
4-Chlorophenyl phenyl ether
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
4-Nitroaniline
<0.029
0.34
0.029 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
4,6-Dinitro-2-methylphenol
<0.051
0.34
0.051 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
N-Nitrosodiphenylamine
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
4-Bromophenyl phenyl ether
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Hexachlorobenzene
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Phenanthrene
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Anthracene
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Di-n-butyl phthalate
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Fluoranthene
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Pyrene
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Butyl benzyl phthalate
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Benzo[a]anthracene
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Chrysene
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Bis(2-ethylhexyl) phthalate
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Di-n-octyl phthalate
<0.019
0.34
0.019 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Benzo[b]fluoranthene
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Benzo[k]fluoranthene
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Benzo[a]pyrene
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Indeno[1,2,3-cd]pyrene
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Dibenz(a,h)anthracene
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Benzo[g,h,i]perylene
<0.017
0.34
0.017 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
3,3'-Dichlorobenzidine
<0.051
0.34
0.051 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
Pentachlorophenol
<0.10
0.34
0.10 mg/Kg
07/25/11 13:21
07/26/11 18:02
1
% Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2-Fluorophenol
72
48
-
130
07/25/11 13:21
